{"data":{"id":"10.6084/m9.figshare.c.3253978.v1","type":"dois","attributes":{"doi":"10.6084/m9.figshare.c.3253978.v1","prefix":"10.6084","suffix":"m9.figshare.c.3253978.v1","identifiers":[],"alternateIdentifiers":[],"creators":[{"name":"Tamasi, Alison L.","nameType":"Personal","givenName":"Alison L.","familyName":"Tamasi","affiliation":[],"nameIdentifiers":[]},{"name":"Pokpong Rungthanapathsophon","affiliation":[],"nameIdentifiers":[]},{"name":"Dame, Ashley N.","nameType":"Personal","givenName":"Ashley N.","familyName":"Dame","affiliation":[],"nameIdentifiers":[]},{"name":"Moody, Morgan A.","nameType":"Personal","givenName":"Morgan A.","familyName":"Moody","affiliation":[],"nameIdentifiers":[]},{"name":"Barnes, Charles L.","nameType":"Personal","givenName":"Charles L.","familyName":"Barnes","affiliation":[],"nameIdentifiers":[]},{"name":"Wilkerson, Marianne P.","nameType":"Personal","givenName":"Marianne P.","familyName":"Wilkerson","affiliation":[],"nameIdentifiers":[]},{"name":"Walensky, Justin R.","nameType":"Personal","givenName":"Justin R.","familyName":"Walensky","affiliation":[],"nameIdentifiers":[]}],"titles":[{"title":"Pseudo-halide uranyl salicylaldiminate complexes including the isolation of a rare uranyl azide"}],"publisher":"Figshare","container":{},"publicationYear":2016,"subjects":[{"subject":"Biophysics"},{"subject":"Biochemistry"},{"subject":"29999 Physical Sciences not elsewhere classified","subjectScheme":"FOR"},{"subject":"FOS: Physical sciences","schemeUri":"http://www.oecd.org/science/inno/38235147.pdf","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"FOS: Physical sciences","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"Medicine"},{"subject":"Microbiology"},{"subject":"FOS: Biological sciences","schemeUri":"http://www.oecd.org/science/inno/38235147.pdf","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"FOS: Biological sciences","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"Genetics"},{"subject":"Molecular Biology"},{"subject":"Biotechnology"},{"subject":"39999 Chemical Sciences not elsewhere classified","subjectScheme":"FOR"},{"subject":"FOS: Chemical sciences","schemeUri":"http://www.oecd.org/science/inno/38235147.pdf","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"FOS: Chemical sciences","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"Sociology"},{"subject":"FOS: Sociology","schemeUri":"http://www.oecd.org/science/inno/38235147.pdf","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"FOS: Sociology","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"80699 Information Systems not elsewhere classified","subjectScheme":"FOR"},{"subject":"FOS: Computer and information sciences","schemeUri":"http://www.oecd.org/science/inno/38235147.pdf","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"FOS: Computer and information sciences","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"Cancer"},{"subject":"Infectious Diseases"},{"subject":"FOS: Health sciences","schemeUri":"http://www.oecd.org/science/inno/38235147.pdf","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"FOS: Health sciences","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"Computational Biology"}],"contributors":[],"dates":[{"date":"2016-05-14","dateType":"Created"},{"date":"2016-06-01","dateType":"Updated"},{"date":"2016","dateType":"Issued"}],"language":null,"types":{"ris":"GEN","bibtex":"misc","citeproc":"article","schemaOrg":"Collection","resourceType":"Collection","resourceTypeGeneral":"Collection"},"relatedIdentifiers":[{"relationType":"IsSupplementTo","relatedIdentifier":"10.1080/00958972.2016.1189544","relatedIdentifierType":"DOI"},{"relationType":"IsIdenticalTo","relatedIdentifier":"10.6084/m9.figshare.c.3253978","relatedIdentifierType":"DOI"}],"relatedItems":[],"sizes":[],"formats":[],"version":null,"rightsList":[{"rights":"CC-BY","rightsUri":"http://creativecommons.org/licenses/by/3.0/us"}],"descriptions":[{"description":"We report the synthesis and spectroscopy of pseudo-halide complexes of uranyl coordinated to salicylaldiminate ligands. The reaction of [(NC\u003csub\u003e9\u003c/sub\u003eH\u003csub\u003e6\u003c/sub\u003e)N=C(H)C\u003csub\u003e6\u003c/sub\u003eH\u003csub\u003e2\u003c/sub\u003e\u003csup\u003e\u003ci\u003et\u003c/i\u003e\u003c/sup\u003eBu\u003csub\u003e2\u003c/sub\u003eO-κ\u003csup\u003e3\u003c/sup\u003e(O,N,N′)]UO\u003csub\u003e2\u003c/sub\u003eCl(THF), \u003cb\u003e1\u003c/b\u003e, with NaN\u003csub\u003e3\u003c/sub\u003e produces a rare example of an uranyl azide, [(NC\u003csub\u003e9\u003c/sub\u003eH\u003csub\u003e6\u003c/sub\u003e)N=C(H)C\u003csub\u003e6\u003c/sub\u003eH\u003csub\u003e2\u003c/sub\u003e\u003csup\u003e\u003ci\u003et\u003c/i\u003e\u003c/sup\u003eBu\u003csub\u003e2\u003c/sub\u003eO-κ\u003csup\u003e3\u003c/sup\u003e(O,N,N′)]UO\u003csub\u003e2\u003c/sub\u003e(N\u003csub\u003e3\u003c/sub\u003e)(THF), \u003cb\u003e2\u003c/b\u003e. A series of isocyanates, [(NC\u003csub\u003e9\u003c/sub\u003eH\u003csub\u003e6\u003c/sub\u003e)N=C(H)C\u003csub\u003e6\u003c/sub\u003eH\u003csub\u003e2\u003c/sub\u003e\u003csup\u003e\u003ci\u003et\u003c/i\u003e\u003c/sup\u003eBu\u003csub\u003e2\u003c/sub\u003eO-κ\u003csup\u003e3\u003c/sup\u003e(O,N,N′)]UO\u003csub\u003e2\u003c/sub\u003e(NCE)(THF), E = O, \u003cb\u003e3\u003c/b\u003e; S, \u003cb\u003e4\u003c/b\u003e; Se, \u003cb\u003e5\u003c/b\u003e, were synthesized from reaction of \u003cb\u003e1\u003c/b\u003e with KNCE. Reaction of \u003cb\u003e1\u003c/b\u003e with AgNO\u003csub\u003e3\u003c/sub\u003e and AgOTf (OTf = SO\u003csub\u003e3\u003c/sub\u003eCF\u003csub\u003e3\u003c/sub\u003e) produces [(NC\u003csub\u003e9\u003c/sub\u003eH\u003csub\u003e6\u003c/sub\u003e)N=C(H)C\u003csub\u003e6\u003c/sub\u003eH\u003csub\u003e2\u003c/sub\u003e\u003csup\u003e\u003ci\u003et\u003c/i\u003e\u003c/sup\u003eBu\u003csub\u003e2\u003c/sub\u003eO-κ\u003csup\u003e3\u003c/sup\u003e(O,N,N′)]UO\u003csub\u003e2\u003c/sub\u003e(NO\u003csub\u003e3\u003c/sub\u003e), \u003cb\u003e6\u003c/b\u003e and [(NC\u003csub\u003e9\u003c/sub\u003eH\u003csub\u003e6\u003c/sub\u003e)N=C(H)C\u003csub\u003e6\u003c/sub\u003eH\u003csub\u003e2\u003c/sub\u003e\u003csup\u003e\u003ci\u003et\u003c/i\u003e\u003c/sup\u003eBu\u003csub\u003e2\u003c/sub\u003eO-κ\u003csup\u003e3\u003c/sup\u003e(O,N,N′)]UO\u003csub\u003e2\u003c/sub\u003e(OTf)(THF), \u003cb\u003e7\u003c/b\u003e, respectively. The newly formed complexes, \u003cb\u003e2\u003c/b\u003e–\u003cb\u003e7\u003c/b\u003e, have been characterized by \u003csup\u003e1\u003c/sup\u003eH, \u003csup\u003e13\u003c/sup\u003eC, and \u003csup\u003e15\u003c/sup\u003eN NMR (where applicable), as well as IR spectroscopy, and the molecular structure of \u003cb\u003e2\u003c/b\u003e, \u003cb\u003e5\u003c/b\u003e, \u003cb\u003e6\u003c/b\u003e\u003cb\u003e,\u003c/b\u003e and \u003cb\u003e7\u003c/b\u003e have been determined by X-ray crystallography.","descriptionType":"Abstract"}],"geoLocations":[],"fundingReferences":[],"xml":"<?xml version="1.0" encoding="UTF-8"?>
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      <creatorName nameType="Personal">Tamasi, Alison L.</creatorName>
      <givenName>Alison L.</givenName>
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      <creatorName>Pokpong Rungthanapathsophon</creatorName>
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      <creatorName nameType="Personal">Dame, Ashley N.</creatorName>
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      <creatorName nameType="Personal">Barnes, Charles L.</creatorName>
      <givenName>Charles L.</givenName>
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  <titles>
    <title>Pseudo-halide uranyl salicylaldiminate complexes including the isolation of a rare uranyl azide</title>
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  <publicationYear>2016</publicationYear>
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    <subject>Biophysics</subject>
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  <dates>
    <date dateType="Created">2016-05-14</date>
    <date dateType="Updated">2016-06-01</date>
    <date dateType="Issued">2016</date>
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    <description descriptionType="Abstract">We report the synthesis and spectroscopy of pseudo-halide complexes of uranyl coordinated to salicylaldiminate ligands. The reaction of [(NC&lt;sub&gt;9&lt;/sub&gt;H&lt;sub&gt;6&lt;/sub&gt;)N=C(H)C&lt;sub&gt;6&lt;/sub&gt;H&lt;sub&gt;2&lt;/sub&gt;&lt;sup&gt;&lt;i&gt;t&lt;/i&gt;&lt;/sup&gt;Bu&lt;sub&gt;2&lt;/sub&gt;O-κ&lt;sup&gt;3&lt;/sup&gt;(O,N,N′)]UO&lt;sub&gt;2&lt;/sub&gt;Cl(THF), &lt;b&gt;1&lt;/b&gt;, with NaN&lt;sub&gt;3&lt;/sub&gt; produces a rare example of an uranyl azide, [(NC&lt;sub&gt;9&lt;/sub&gt;H&lt;sub&gt;6&lt;/sub&gt;)N=C(H)C&lt;sub&gt;6&lt;/sub&gt;H&lt;sub&gt;2&lt;/sub&gt;&lt;sup&gt;&lt;i&gt;t&lt;/i&gt;&lt;/sup&gt;Bu&lt;sub&gt;2&lt;/sub&gt;O-κ&lt;sup&gt;3&lt;/sup&gt;(O,N,N′)]UO&lt;sub&gt;2&lt;/sub&gt;(N&lt;sub&gt;3&lt;/sub&gt;)(THF), &lt;b&gt;2&lt;/b&gt;. A series of isocyanates, [(NC&lt;sub&gt;9&lt;/sub&gt;H&lt;sub&gt;6&lt;/sub&gt;)N=C(H)C&lt;sub&gt;6&lt;/sub&gt;H&lt;sub&gt;2&lt;/sub&gt;&lt;sup&gt;&lt;i&gt;t&lt;/i&gt;&lt;/sup&gt;Bu&lt;sub&gt;2&lt;/sub&gt;O-κ&lt;sup&gt;3&lt;/sup&gt;(O,N,N′)]UO&lt;sub&gt;2&lt;/sub&gt;(NCE)(THF), E = O, &lt;b&gt;3&lt;/b&gt;; S, &lt;b&gt;4&lt;/b&gt;; Se, &lt;b&gt;5&lt;/b&gt;, were synthesized from reaction of &lt;b&gt;1&lt;/b&gt; with KNCE. Reaction of &lt;b&gt;1&lt;/b&gt; with AgNO&lt;sub&gt;3&lt;/sub&gt; and AgOTf (OTf = SO&lt;sub&gt;3&lt;/sub&gt;CF&lt;sub&gt;3&lt;/sub&gt;) produces [(NC&lt;sub&gt;9&lt;/sub&gt;H&lt;sub&gt;6&lt;/sub&gt;)N=C(H)C&lt;sub&gt;6&lt;/sub&gt;H&lt;sub&gt;2&lt;/sub&gt;&lt;sup&gt;&lt;i&gt;t&lt;/i&gt;&lt;/sup&gt;Bu&lt;sub&gt;2&lt;/sub&gt;O-κ&lt;sup&gt;3&lt;/sup&gt;(O,N,N′)]UO&lt;sub&gt;2&lt;/sub&gt;(NO&lt;sub&gt;3&lt;/sub&gt;), &lt;b&gt;6&lt;/b&gt; and [(NC&lt;sub&gt;9&lt;/sub&gt;H&lt;sub&gt;6&lt;/sub&gt;)N=C(H)C&lt;sub&gt;6&lt;/sub&gt;H&lt;sub&gt;2&lt;/sub&gt;&lt;sup&gt;&lt;i&gt;t&lt;/i&gt;&lt;/sup&gt;Bu&lt;sub&gt;2&lt;/sub&gt;O-κ&lt;sup&gt;3&lt;/sup&gt;(O,N,N′)]UO&lt;sub&gt;2&lt;/sub&gt;(OTf)(THF), &lt;b&gt;7&lt;/b&gt;, respectively. The newly formed complexes, &lt;b&gt;2&lt;/b&gt;–&lt;b&gt;7&lt;/b&gt;, have been characterized by &lt;sup&gt;1&lt;/sup&gt;H, &lt;sup&gt;13&lt;/sup&gt;C, and &lt;sup&gt;15&lt;/sup&gt;N NMR (where applicable), as well as IR spectroscopy, and the molecular structure of &lt;b&gt;2&lt;/b&gt;, &lt;b&gt;5&lt;/b&gt;, &lt;b&gt;6&lt;/b&gt;&lt;b&gt;,&lt;/b&gt; and &lt;b&gt;7&lt;/b&gt; have been determined by X-ray crystallography.</description>
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