{"data":{"id":"10.6084/m9.figshare.c.2859898","type":"dois","attributes":{"doi":"10.6084/m9.figshare.c.2859898","prefix":"10.6084","suffix":"m9.figshare.c.2859898","identifiers":[],"alternateIdentifiers":[],"creators":[{"name":"Yuan, Juan","nameType":"Personal","givenName":"Juan","familyName":"Yuan","affiliation":[],"nameIdentifiers":[]},{"name":"Chu, Yi-Xin","nameType":"Personal","givenName":"Yi-Xin","familyName":"Chu","affiliation":[],"nameIdentifiers":[]},{"name":"Kou, Hui-Zhong","nameType":"Personal","givenName":"Hui-Zhong","familyName":"Kou","affiliation":[],"nameIdentifiers":[]}],"titles":[{"title":"Synthesis, crystal structures, and magnetic properties of methoxido-bridged dinuclear Mn\u003csup\u003eIII\u003c/sup\u003e complexes derived from tri-dentate chelating ligands"}],"publisher":"Figshare","container":{},"publicationYear":2016,"subjects":[{"subject":"Biochemistry"},{"subject":"29999 Physical Sciences not elsewhere classified","subjectScheme":"FOR"},{"subject":"FOS: Physical sciences","schemeUri":"http://www.oecd.org/science/inno/38235147.pdf","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"FOS: Physical sciences","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"Cell Biology"},{"subject":"Molecular Biology"},{"subject":"Physiology"},{"subject":"FOS: Biological sciences","schemeUri":"http://www.oecd.org/science/inno/38235147.pdf","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"FOS: Biological sciences","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"Pharmacology"},{"subject":"Biotechnology"},{"subject":"39999 Chemical Sciences not elsewhere classified","subjectScheme":"FOR"},{"subject":"FOS: Chemical sciences","schemeUri":"http://www.oecd.org/science/inno/38235147.pdf","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"FOS: Chemical sciences","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"Developmental Biology"},{"subject":"Plant Biology"}],"contributors":[],"dates":[{"date":"2016-03-23","dateType":"Created"},{"date":"2016-05-28","dateType":"Updated"},{"date":"2016","dateType":"Issued"}],"language":null,"types":{"ris":"GEN","bibtex":"misc","citeproc":"article","schemaOrg":"Collection","resourceType":"Collection","resourceTypeGeneral":"Collection"},"relatedIdentifiers":[{"relationType":"IsSupplementTo","relatedIdentifier":"10.1080/00958972.2016.1166217","relatedIdentifierType":"DOI"}],"relatedItems":[],"sizes":[],"formats":[],"version":null,"rightsList":[{"rights":"CC-BY","rightsUri":"http://creativecommons.org/licenses/by/3.0/us"}],"descriptions":[{"description":"Two new doubly methoxido-bridged Mn\u003csup\u003eIII\u003c/sup\u003e dinuclear complexes, [Mn\u003csup\u003eIII\u003c/sup\u003e(mphp)(\u003ci\u003eμ\u003c/i\u003e-OCH\u003csub\u003e3\u003c/sub\u003e)(CH\u003csub\u003e3\u003c/sub\u003eOH)]\u003csub\u003e2\u003c/sub\u003e·2CH\u003csub\u003e3\u003c/sub\u003eOH (\u003cb\u003e1\u003c/b\u003e) and ([Mn\u003csup\u003eIII\u003c/sup\u003e(ahbz)(\u003ci\u003eμ\u003c/i\u003e-OCH\u003csub\u003e3\u003c/sub\u003e)(CH\u003csub\u003e3\u003c/sub\u003eOH)]\u003csub\u003e2\u003c/sub\u003e·2CH\u003csub\u003e3\u003c/sub\u003eOH (\u003cb\u003e2\u003c/b\u003e), have been synthesized by using the tridentate ligands H\u003csub\u003e2\u003c/sub\u003emphp (H\u003csub\u003e2\u003c/sub\u003emph\u003ci\u003ep\u003c/i\u003e = 2-methyl-6-(pyrimidin-2-yl-hydrazonomethyl)-phenol) and H\u003csub\u003e2\u003c/sub\u003eahbz (H\u003csub\u003e2\u003c/sub\u003eahbz = N-(2-amino-propyl)-2-hydroxy-benzamide). The complexes have been characterized by single-crystal X-ray diffraction analysis and magnetic measurements. Complexes \u003cb\u003e1\u003c/b\u003e and \u003cb\u003e2\u003c/b\u003e have a similar dimeric molecular structure. Two [Mn(L)(CH\u003csub\u003e3\u003c/sub\u003eOH)]\u003csup\u003e+\u003c/sup\u003e moieties (L\u003csup\u003e2−\u003c/sup\u003e = mphp\u003csup\u003e2−\u003c/sup\u003e or ahbz\u003csup\u003e2−\u003c/sup\u003e) are bridged by two \u003ci\u003eμ\u003c/i\u003e-OCH\u003csub\u003e3\u003c/sub\u003e\u003csup\u003e−\u003c/sup\u003e groups in the axial-equatorial asymmetric manner. The coordination geometry of Mn\u003csup\u003eIII\u003c/sup\u003e is an axially elongated octahedron with two oxygens of a methanol ligand and a methoxido ligand situated at the axial positions. Magnetic measurements indicate that \u003cb\u003e1\u003c/b\u003e and \u003cb\u003e2\u003c/b\u003e exhibit antiferromagnetic behavior with the fitting parameter of \u003ci\u003eJ\u003c/i\u003e = −1.49(3) cm\u003csup\u003e−1\u003c/sup\u003e, \u003ci\u003eD\u003c/i\u003e = −1.3(1) cm\u003csup\u003e−1\u003c/sup\u003e, \u003ci\u003eg\u003c/i\u003e = 1.98(1) and \u003ci\u003ezJ\u003c/i\u003e′ = −0.18(4) cm\u003csup\u003e−1\u003c/sup\u003e for \u003cb\u003e1\u003c/b\u003e, and \u003ci\u003eJ\u003c/i\u003e = −1.6(2) cm\u003csup\u003e−1\u003c/sup\u003e, \u003ci\u003eD\u003c/i\u003e = 4.5(3) cm\u003csup\u003e−1\u003c/sup\u003e, \u003ci\u003eg\u003c/i\u003e = 2.06(1) and \u003ci\u003ezJ\u003c/i\u003e′ = 1.4(1) cm\u003csup\u003e−1\u003c/sup\u003e for \u003cb\u003e2\u003c/b\u003e on the basis of the spin Hamiltonian \u003ci\u003eĤ\u003c/i\u003e = −2\u003ci\u003eJŜ\u003c/i\u003e\u003csub\u003eMn1\u003c/sub\u003e\u003ci\u003eŜ\u003c/i\u003e\u003csub\u003eMn2\u003c/sub\u003e.","descriptionType":"Abstract"}],"geoLocations":[],"fundingReferences":[],"xml":"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