{"data":{"id":"10.6084/m9.figshare.c.2037488","type":"dois","attributes":{"doi":"10.6084/m9.figshare.c.2037488","prefix":"10.6084","suffix":"m9.figshare.c.2037488","identifiers":[],"alternateIdentifiers":[],"creators":[{"name":"Li, Tao","givenName":"Tao","familyName":"Li","affiliation":[],"nameIdentifiers":[]},{"name":"Mei, Mei","givenName":"Mei","familyName":"Mei","affiliation":[],"nameIdentifiers":[]},{"name":"Gao, Hongjun","givenName":"Hongjun","familyName":"Gao","affiliation":[],"nameIdentifiers":[]},{"name":"Li, Yuanqiang","givenName":"Yuanqiang","familyName":"Li","affiliation":[],"nameIdentifiers":[]},{"name":"Yan, Yongliang","givenName":"Yongliang","familyName":"Yan","affiliation":[],"nameIdentifiers":[]},{"name":"Che, Daqing","givenName":"Daqing","familyName":"Che","affiliation":[],"nameIdentifiers":[]}],"titles":[{"title":"Thionyl Chloride–Mediated Synthesis of \u003ci\u003etert\u003c/i\u003e-Butyl ((\u003ci\u003eS\u003c/i\u003e)-1-((\u003ci\u003eR\u003c/i\u003e)-Oxiran-2-yl)-2-phenylethyl)carbamate with Boc-Involved Neighboring Group Participation"}],"publisher":"Taylor \u0026 Francis","container":{},"publicationYear":2015,"subjects":[{"subject":"Science Policy"},{"subject":"Developmental Biology"},{"subject":"Biological Sciences"},{"subject":"Immunology"},{"subject":"FOS: Clinical medicine","schemeUri":"http://www.oecd.org/science/inno/38235147.pdf","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"Earth and Environmental Sciences"},{"subject":"Physiology"},{"subject":"FOS: Biological sciences","schemeUri":"http://www.oecd.org/science/inno/38235147.pdf","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"Cell Biology"},{"subject":"Microbiology"},{"subject":"Biochemistry"}],"contributors":[],"dates":[{"date":"2015-12-05","dateType":"Created"},{"date":"2019-08-19","dateType":"Updated"},{"date":"2015","dateType":"Issued"}],"language":null,"types":{"ris":"GEN","bibtex":"misc","citeproc":"article","schemaOrg":"Collection","resourceType":"Collection","resourceTypeGeneral":"Collection"},"relatedIdentifiers":[],"relatedItems":[],"sizes":[],"formats":[],"version":null,"rightsList":[{"rights":"Creative Commons Attribution 4.0 International","rightsUri":"https://creativecommons.org/licenses/by/4.0/legalcode","schemeUri":"https://spdx.org/licenses/","rightsIdentifier":"cc-by-4.0","rightsIdentifierScheme":"SPDX"}],"descriptions":[{"description":"A convenient, high-yielding preparation of \u003ci\u003etert\u003c/i\u003e-butyl ((\u003ci\u003eS\u003c/i\u003e)-1-((\u003ci\u003eR\u003c/i\u003e)-oxiran-2-yl)-2-phenylethyl)carbamate is described. An efficient chiral inversion as the key step is furnished via Boc-involved neighboring group participation mediated by thionyl chloride. This preparation has significant advantages over the previously reported methods with respect to simplicity, cost efficiency, yield, and purification procedure as well as industry 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