{"data":{"id":"10.6084/m9.figshare.825653","type":"dois","attributes":{"doi":"10.6084/m9.figshare.825653","prefix":"10.6084","suffix":"m9.figshare.825653","identifiers":[],"alternateIdentifiers":[],"creators":[{"name":"Marivil D. Islam","affiliation":[],"nameIdentifiers":[]},{"name":"Haberhauer, Georg","nameType":"Personal","givenName":"Georg","familyName":"Haberhauer","affiliation":[],"nameIdentifiers":[]},{"name":"Kist, Alla","nameType":"Personal","givenName":"Alla","familyName":"Kist","affiliation":[],"nameIdentifiers":[]},{"name":"M. Nasir Rathor","affiliation":[],"nameIdentifiers":[]},{"name":"Gerzabek, Martin","nameType":"Personal","givenName":"Martin","familyName":"Gerzabek","affiliation":[],"nameIdentifiers":[]},{"name":"Cannavan, Andrew","nameType":"Personal","givenName":"Andrew","familyName":"Cannavan","affiliation":[],"nameIdentifiers":[]}],"titles":[{"title":"Multi-class determination of anthelmintics in soil and water by LC-MS/MS"}],"publisher":"Taylor \u0026 Francis","container":{},"publicationYear":2013,"subjects":[{"subject":"Microbiology"},{"subject":"FOS: Biological sciences","schemeUri":"http://www.oecd.org/science/inno/38235147.pdf","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"FOS: Biological sciences","subjectScheme":"Fields of Science and Technology (FOS)"}],"contributors":[],"dates":[{"date":"2013-10-17","dateType":"Created"},{"date":"2013-10-21","dateType":"Updated"},{"date":"2013","dateType":"Issued"}],"language":null,"types":{"ris":"DATA","bibtex":"misc","citeproc":"dataset","schemaOrg":"Dataset","resourceType":"Dataset","resourceTypeGeneral":"Dataset"},"relatedIdentifiers":[{"relationType":"IsSupplementTo","relatedIdentifier":"10.1080/19440049.2013.777974","relatedIdentifierType":"DOI"}],"relatedItems":[],"sizes":["104088 Bytes"],"formats":[],"version":null,"rightsList":[{"rights":"Creative Commons Attribution 4.0 International","rightsUri":"https://creativecommons.org/licenses/by/4.0/legalcode","schemeUri":"https://spdx.org/licenses/","rightsIdentifier":"cc-by-4.0","rightsIdentifierScheme":"SPDX"}],"descriptions":[{"description":"The translocation of antiparasitic drugs from animal excrement through soil and water to crops and forages and their recycling to food-producing animals is a potential concern with respect to the contamination of the food chain. To facilitate the investigation of this problem, an LC-MS/MS method for selected anthelmintics in soil and water was developed. The soil sample preparation involved a simple solvent extraction and dispersive clean-up technique. The method was validated at 10, 20 and 40 µg kg\u003csup\u003e−1\u003c/sup\u003e for levamisole, fenbendazole, fenbendazole sulphoxide and fenbendazole sulphone and at 20, 40 and 80 µg kg\u003csup\u003e−1\u003c/sup\u003e for eprinomectin. LOQs were 10 µg kg\u003csup\u003e−1\u003c/sup\u003e for the first four compounds and 20 µg kg\u003csup\u003e−1\u003c/sup\u003e for eprinomectin. The overall mean recoveries ranged from 76.1% to 89% for loamy soils and from 79.9% to 96.9% for sandy soils. Analysis of water samples was performed by extraction/concentration on an Oasis-HLB (Aschaffenburg, Germany) cartridge. Validation was performed at 0.25, 0.5 and 1.0 µg l\u003csup\u003e−1\u003c/sup\u003e. The LOQ for all compounds was 0.25 µg l\u003csup\u003e−1\u003c/sup\u003e. Method recovery (and RSD) varied between 35.4% (28) for eprinomectin and 125.1% (16) for fenbendazole sulphone. The validated methods were applied to soil and water samples in a study on the behaviour of anthelmintic drugs in a soil-plant-water system (manuscript on “transport investigation of antiparasitic drugs based on a lysimeter experiment” in preparation).","descriptionType":"Abstract"}],"geoLocations":[],"fundingReferences":[],"xml":"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","url":"https://tandf.figshare.com/articles/dataset/Multi_class_determination_of_anthelmintics_in_soil_and_water_by_LC_MS_MS/825653","contentUrl":null,"metadataVersion":3,"schemaVersion":"http://datacite.org/schema/kernel-4","source":"mds","isActive":true,"state":"findable","reason":null,"viewCount":0,"viewsOverTime":[],"downloadCount":0,"downloadsOverTime":[],"referenceCount":0,"citationCount":0,"citationsOverTime":[],"partCount":0,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