{"data":{"id":"10.6084/m9.figshare.7046123","type":"dois","attributes":{"doi":"10.6084/m9.figshare.7046123","prefix":"10.6084","suffix":"m9.figshare.7046123","identifiers":[],"alternateIdentifiers":[],"creators":[{"name":"Magalhães, Gabriela Oliveira De","nameType":"Personal","givenName":"Gabriela Oliveira De","familyName":"Magalhães","affiliation":[],"nameIdentifiers":[]},{"name":"Jéssica De Oliveira Notório Ribeiro","affiliation":[],"nameIdentifiers":[]},{"name":"Vasconcelos, Daniela Cordeiro Leite","nameType":"Personal","givenName":"Daniela Cordeiro Leite","familyName":"Vasconcelos","affiliation":[],"nameIdentifiers":[]},{"name":"Vasconcelos, Wander Luiz","nameType":"Personal","givenName":"Wander Luiz","familyName":"Vasconcelos","affiliation":[],"nameIdentifiers":[]}],"titles":[{"title":"Production of Pure Granules Of Sba-15 Mesoporous Silica"}],"publisher":"SciELO journals","container":{},"publicationYear":2018,"subjects":[{"subject":"90499 Chemical Engineering not elsewhere classified","subjectScheme":"FOR"},{"subject":"FOS: Chemical engineering","schemeUri":"http://www.oecd.org/science/inno/38235147.pdf","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"FOS: Chemical engineering","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"91207 Metals and Alloy Materials","subjectScheme":"FOR"},{"subject":"FOS: Materials engineering","schemeUri":"http://www.oecd.org/science/inno/38235147.pdf","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"FOS: Materials engineering","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"91299 Materials Engineering not elsewhere classified","subjectScheme":"FOR"}],"contributors":[],"dates":[{"date":"2018-09-05","dateType":"Created"},{"date":"2018-09-05","dateType":"Updated"},{"date":"2018","dateType":"Issued"}],"language":null,"types":{"ris":"DATA","bibtex":"misc","citeproc":"dataset","schemaOrg":"Dataset","resourceType":"Dataset","resourceTypeGeneral":"Dataset"},"relatedIdentifiers":[{"relationType":"IsSupplementTo","relatedIdentifier":"10.1590/1980-5373-mr-2018-0148","relatedIdentifierType":"DOI"}],"relatedItems":[],"sizes":["1761712 Bytes"],"formats":[],"version":null,"rightsList":[{"rights":"Creative Commons Attribution 4.0 International","rightsUri":"https://creativecommons.org/licenses/by/4.0/legalcode","schemeUri":"https://spdx.org/licenses/","rightsIdentifier":"cc-by-4.0","rightsIdentifierScheme":"SPDX"}],"descriptions":[{"description":"Mesoporous silica materials have been widely investigated for their great potential as competitive adsorbents and catalysts in different areas, due to their ordered and uniform porous structures and high surface area. In order to increase the availability of these materials, the need to granulate them becomes vital for an efficient performance in industrial units. This study reports the production and characterization of clay-free granules of SBA-15 mesoporous silica, by applying the extrusion technique. The suggested methodology uses only methocel as the organic binder, which is removed after calcination. The granulation process was successfully achieved, producing pure granules of SBA-15 mesoporous silica, in size of millimeters, with 8.3 MPa of compacting pressure (by axial crushing test). The surface area and pore volume of SBA-15 mesoporous silica granules (calcined at 800 ºC) were around 392 m2/g and 0.53 cm3/g, respectively.","descriptionType":"Abstract"}],"geoLocations":[],"fundingReferences":[],"xml":"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","url":"https://scielo.figshare.com/articles/Production_of_Pure_Granules_Of_Sba-15_Mesoporous_Silica/7046123","contentUrl":null,"metadataVersion":2,"schemaVersion":"http://datacite.org/schema/kernel-4","source":"mds","isActive":true,"state":"findable","reason":null,"viewCount":0,"viewsOverTime":[],"downloadCount":0,"downloadsOverTime":[],"referenceCount":1,"citationCount":0,"citationsOverTime":[],"partCount":0,"partOfCount":0,"versionCount":0,"versionOfCount":0,"created":"2018-09-05T02:49:40.000Z","registered":"2018-09-05T02:50:42.000Z","published":"2018","updated":"2020-08-28T11:34:50.000Z"},"relationships":{"client":{"data":{"id":"figshare.ars","type":"clients"}},"provider":{"data":{"id":"otjm","type":"providers"}},"media":{"data":{"id":"10.6084/m9.figshare.7046123","type":"media"}},"references":{"data":[{"id":"10.1590/1980-5373-mr-2018-0148","type":"dois"}]},"citations":{"data":[]},"parts":{"data":[]},"partOf":{"data":[]},"versions":{"data":[]},"versionOf":{"data":[]}}}}