{"data":{"id":"10.6084/m9.figshare.6856931.v1","type":"dois","attributes":{"doi":"10.6084/m9.figshare.6856931.v1","prefix":"10.6084","suffix":"m9.figshare.6856931.v1","identifiers":[],"alternateIdentifiers":[],"creators":[{"name":"Eckerdt, Carolina López","nameType":"Personal","givenName":"Carolina López","familyName":"Eckerdt","affiliation":[],"nameIdentifiers":[]},{"name":"Sanabria, Ricardo Martín","nameType":"Personal","givenName":"Ricardo Martín","familyName":"Sanabria","affiliation":[],"nameIdentifiers":[]},{"name":"Peitsch, Pablo Edgardo Reynoso","nameType":"Personal","givenName":"Pablo Edgardo Reynoso","familyName":"Peitsch","affiliation":[],"nameIdentifiers":[]},{"name":"Mirandou, Marcela Inés","nameType":"Personal","givenName":"Marcela Inés","familyName":"Mirandou","affiliation":[],"nameIdentifiers":[]},{"name":"Aricó, Sergio Fabián","nameType":"Personal","givenName":"Sergio Fabián","familyName":"Aricó","affiliation":[],"nameIdentifiers":[]}],"titles":[{"title":"Study of the U3Si5, USi2-x and USi2 phases stability due to the incorporation of aluminium in solution by the use of Differential Scanning Calorimetry (DSC) technique"}],"publisher":"SciELO journals","container":{},"publicationYear":2018,"subjects":[{"subject":"90502 Construction Engineering","subjectScheme":"FOR"},{"subject":"FOS: Civil engineering","schemeUri":"http://www.oecd.org/science/inno/38235147.pdf","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"FOS: Civil engineering","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"91207 Metals and Alloy Materials","subjectScheme":"FOR"},{"subject":"FOS: Materials engineering","schemeUri":"http://www.oecd.org/science/inno/38235147.pdf","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"FOS: Materials engineering","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"91299 Materials Engineering not elsewhere classified","subjectScheme":"FOR"}],"contributors":[],"dates":[{"date":"2018-07-25","dateType":"Created"},{"date":"2018-07-25","dateType":"Updated"},{"date":"2018","dateType":"Issued"}],"language":null,"types":{"ris":"DATA","bibtex":"misc","citeproc":"dataset","schemaOrg":"Dataset","resourceType":"Dataset","resourceTypeGeneral":"Dataset"},"relatedIdentifiers":[{"relationType":"IsSupplementTo","relatedIdentifier":"10.1590/s1517-707620180002.0437","relatedIdentifierType":"DOI"},{"relationType":"IsIdenticalTo","relatedIdentifier":"10.6084/m9.figshare.6856931","relatedIdentifierType":"DOI"}],"relatedItems":[],"sizes":["1053962 Bytes"],"formats":[],"version":null,"rightsList":[{"rights":"Creative Commons Attribution 4.0 International","rightsUri":"https://creativecommons.org/licenses/by/4.0/legalcode","schemeUri":"https://spdx.org/licenses/","rightsIdentifier":"cc-by-4.0","rightsIdentifierScheme":"SPDX"}],"descriptions":[{"description":"ABSTRACT U(Mo) alloys are being studied to be applied as a fuel for research and test reactors. When U(Mo) particles are dispersed in an Al matrix, it is known that an interdiffusion during fabrication process and / or irradiation. In this sense, irradiation tests have shown that this IL has a bad behavior under irradiation coming up the addition of Si to Al as one of the most promising solutions. Several out of pile experiences have been performed with U(Mo)/Al(Si) diffusion couples in which U(Al,SI)3, U3Si5, USi2, USi2-x, Al20Mo2U and/or Al43Mo4U6 are the phases identified as conforming the IL. In some cases, U3Si5 was identified considering modified lattice parameters, which can be justified assuming that the U3Si5 phase would accept a small amount of Al in solution. However, although the Al-Si-U ternary system has been extensively studied, there are no previous experimental results to correlate lattice parameters modification with Al solubility in U3Si5, USi2 y USi2-x phases. From previous paragraphs, it is important to study the Al-Si-U ternary system especially in the environment of U3Si5, USi2 and USi2-x phases. With this aim, ten alloys were fabricated. Nine of them were isothermally treated at 550 ºC and microstructurally characterized. The Main results show the presence of needle-like morphology in the alloys with concentrations around that of the U3Si5 phase. From th fact that this kind of morphologies is characteristic of a displacive transformation, which occur during cooling process, the use of a dynamic identification transformation technique (as differential scanning calorimetry) came up as mandatory in this research In this new stage, nine alloys were studied with the calorimeter using two heating/coolig rates (± 1 ºC/min and ± 10 ºC/min). Transformation temperatures and enthalpy of formation of compounds were determined. The samples were also microstructurally characterized after testing.","descriptionType":"Abstract"}],"geoLocations":[],"fundingReferences":[],"xml":"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","url":"https://scielo.figshare.com/articles/Study_of_the_U3Si5_USi2-x_and_USi2_phases_stability_due_to_the_incorporation_of_aluminium_in_solution_by_the_use_of_Differential_Scanning_Calorimetry_DSC_technique/6856931/1","contentUrl":null,"metadataVersion":2,"schemaVersion":"http://datacite.org/schema/kernel-4","source":"mds","isActive":true,"state":"findable","reason":null,"viewCount":0,"viewsOverTime":[],"downloadCount":0,"downloadsOverTime":[],"referenceCount":1,"citationCount":0,"citationsOverTime":[],"partCount":0,"partOfCount":0,"versionCount":0,"versionOfCount":0,"created":"2018-07-25T02:40:31.000Z","registered":"2018-07-25T02:41:52.000Z","published":"2018","updated":"2020-08-28T16:27:51.000Z"},"relationships":{"client":{"data":{"id":"figshare.ars","type":"clients"}},"provider":{"data":{"id":"otjm","type":"providers"}},"media":{"data":{"id":"10.6084/m9.figshare.6856931.v1","type":"media"}},"references":{"data":[{"id":"10.1590/s1517-707620180002.0437","type":"dois"}]},"citations":{"data":[]},"parts":{"data":[]},"partOf":{"data":[]},"versions":{"data":[]},"versionOf":{"data":[]}}}}