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No significant corrosion of the Cu electrode was found while synthesizing from AS in presence of H\u003csub\u003e2\u003c/sub\u003eSO\u003csub\u003e4\u003c/sub\u003e, whereas relatively higher corrosion of Cu as well as contamination of synthesized PAni with corroded Cu were observed for the synthesis from aniline in presence of H\u003csub\u003e2\u003c/sub\u003eSO\u003csub\u003e4\u003c/sub\u003e or from AS in the absence of H\u003csub\u003e2\u003c/sub\u003eSO\u003csub\u003e4\u003c/sub\u003e. Corrosion-free synthesis yields PAni free from contamination of Cu and exhibits smaller particle size and superior electrical and supercapacitive behavior compared to the process exhibiting corrosion of counter electrode.","descriptionType":"Abstract"}],"geoLocations":[],"fundingReferences":[],"xml":"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","url":"https://tandf.figshare.com/articles/dataset/Corrosion_Free_Electrochemical_Synthesis_of_Polyaniline_Using_Cu_Counter_Electrode_in_Acidic_Medium/3085726/2","contentUrl":null,"metadataVersion":2,"schemaVersion":"http://datacite.org/schema/kernel-4","source":"mds","isActive":true,"state":"findable","reason":null,"viewCount":0,"viewsOverTime":[],"downloadCount":0,"downloadsOverTime":[],"referenceCount":1,"citationCount":0,"citationsOverTime":[],"partCount":0,"partOfCount":0,"versionCount":0,"versionOfCount":0,"created":"2016-04-11T18:09:57.000Z","registered":"2016-04-11T18:09:58.000Z","published":"2016","updated":"2020-09-04T12:34:27.000Z"},"relationships":{"client":{"data":{"id":"figshare.ars","type":"clients"}},"provider":{"data":{"id":"otjm","type":"providers"}},"media":{"data":{"id":"10.6084/m9.figshare.3085726.v2","type":"media"}},"references":{"data":[{"id":"10.1080/00914037.2016.1149842",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