{"data":{"id":"10.6084/m9.figshare.1393412","type":"dois","attributes":{"doi":"10.6084/m9.figshare.1393412","prefix":"10.6084","suffix":"m9.figshare.1393412","identifiers":[],"alternateIdentifiers":[],"creators":[{"name":"Huanhuan Wu","affiliation":[],"nameIdentifiers":[]},{"name":"Haijuan Du","affiliation":[],"nameIdentifiers":[]},{"name":"Yunyin Niu","affiliation":[],"nameIdentifiers":[]},{"name":"Zunzhe Shu","affiliation":[],"nameIdentifiers":[]},{"name":"Lixia Shen","affiliation":[],"nameIdentifiers":[]}],"titles":[{"title":"Synthesis and Crystal Structure of an Inorganic-Organic Hybrid Material: [1,1′-dibutyl-4,4′-bipyridinium][α-Mo\u003csub\u003e8\u003c/sub\u003eO\u003csub\u003e26\u003c/sub\u003e]\u003csub\u003e0.5\u003c/sub\u003e"}],"publisher":"Taylor \u0026 Francis","container":{},"publicationYear":2015,"subjects":[{"subject":"110309 Infectious Diseases","subjectScheme":"FOR"},{"subject":"FOS: Health sciences","schemeUri":"http://www.oecd.org/science/inno/38235147.pdf","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"FOS: Health sciences","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"Biological Sciences"},{"subject":"Ecology"},{"subject":"FOS: Biological sciences","schemeUri":"http://www.oecd.org/science/inno/38235147.pdf","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"FOS: Biological sciences","subjectScheme":"Fields of Science and Technology (FOS)"},{"subject":"Chemistry"},{"subject":"Biotechnology"},{"subject":"Molecular Biology"},{"subject":"Cell Biology"},{"subject":"Microbiology"},{"subject":"Biochemistry"}],"contributors":[],"dates":[{"date":"2015-04-24","dateType":"Created"},{"date":"2015-04-24","dateType":"Updated"},{"date":"2015","dateType":"Issued"}],"language":null,"types":{"ris":"DATA","bibtex":"misc","citeproc":"dataset","schemaOrg":"Dataset","resourceType":"Dataset","resourceTypeGeneral":"Dataset"},"relatedIdentifiers":[{"relationType":"IsSupplementTo","relatedIdentifier":"10.1080/15533174.2013.862702","relatedIdentifierType":"DOI"}],"relatedItems":[],"sizes":["26344 Bytes"],"formats":[],"version":null,"rightsList":[{"rights":"Creative Commons Attribution 4.0 International","rightsUri":"https://creativecommons.org/licenses/by/4.0/legalcode","schemeUri":"https://spdx.org/licenses/","rightsIdentifier":"cc-by-4.0","rightsIdentifierScheme":"SPDX"}],"descriptions":[{"description":"A novel inorganic–organic hybrid polyoxometalate, [1,1′-dibutyl-4,4′-bipyridinium,][α-Mo\u003csub\u003e8\u003c/sub\u003eO\u003csub\u003e26\u003c/sub\u003e]\u003csub\u003e0.5\u003c/sub\u003e (\u003cb\u003e1\u003c/b\u003e), has been synthesized by the cation-templated self-assembly with octamolybdate anions under hydrothermal reaction conditions. The structure has been determined by single-crystal X-ray diffraction analysis and further characterized by PXRD, IR spectra, and elemental analysis. The crystal data analysis revealed that the compound was composed of one discrete [1,1′-dibutyl-4′-bipyridinium]\u003csup\u003e2+\u003c/sup\u003e cation and 0.5 polyacid anions [Mo\u003csub\u003e8\u003c/sub\u003eO\u003csub\u003e26\u003c/sub\u003e]\u003csup\u003e4–\u003c/sup\u003e interacted by electrostatic interactions. In the compound the anion fraction take on a [α-Mo\u003csub\u003e8\u003c/sub\u003eO\u003csub\u003e26\u003c/sub\u003e]\u003csup\u003e4–\u003c/sup\u003e cluster.","descriptionType":"Abstract"}],"geoLocations":[],"fundingReferences":[],"xml":"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","url":"https://tandf.figshare.com/articles/dataset/Synthesis_and_Crystal_Structure_of_an_Inorganic_Organic_Hybrid_Material_1_1_dibutyl_4_4_bipyridinium_Mo_sub_8_sub_O_sub_26_sub_sub_0_5_sub_/1393412","contentUrl":null,"metadataVersion":2,"schemaVersion":"http://datacite.org/schema/kernel-4","source":"mds","isActive":true,"state":"findable","reason":null,"viewCount":0,"viewsOverTime":[],"downloadCount":0,"downloadsOverTime":[],"referenceCount":0,"citationCount":0,"citationsOverTime":[],"partCount":0,"partOfCount":0,"versionCount":0,"versionOfCount":0,"created":"2015-04-24T20:49:06.000Z","registered":"2015-04-24T20:49:07.000Z","published":"2015","updated":"2020-09-04T17:54:07.000Z"},"relationships":{"client":{"data":{"id":"figshare.ars","type":"clie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