{"data":{"id":"10.5061/dryad.v9s4mw6tm","type":"dois","attributes":{"doi":"10.5061/dryad.v9s4mw6tm","prefix":"10.5061","suffix":"dryad.v9s4mw6tm","identifiers":[],"alternateIdentifiers":[],"creators":[{"name":"Hu, Jiayang","nameType":"Personal","givenName":"Jiayang","familyName":"Hu","affiliation":["Columbia University"],"nameIdentifiers":[{"schemeUri":"https://orcid.org","nameIdentifier":"https://orcid.org/0000-0001-6707-1549","nameIdentifierScheme":"ORCID"}]},{"name":"Pan, Brady","nameType":"Personal","givenName":"Brady","familyName":"Pan","affiliation":["Columbia University"],"nameIdentifiers":[]},{"name":"Makihara, Takuma","nameType":"Personal","givenName":"Takuma","familyName":"Makihara","affiliation":["Rice University"],"nameIdentifiers":[]},{"name":"Garcia, Roy D. J.","nameType":"Personal","givenName":"Roy D. J.","familyName":"Garcia","affiliation":["Columbia University"],"nameIdentifiers":[]},{"name":"Herman, Irving P.","nameType":"Personal","givenName":"Irving P.","familyName":"Herman","affiliation":["Columbia University"],"nameIdentifiers":[]}],"titles":[{"title":"Brewster angle optical reflection observation of self-limiting nanoparticle monolayer self-assembly at a liquid/liquid interface"}],"publisher":"Dryad","container":{},"publicationYear":2021,"subjects":[{"subject":"FOS: Nano-technology","schemeUri":"https://web-archive.oecd.org/2012-06-15/138575-38235147.pdf","subjectScheme":"fos"}],"contributors":[],"dates":[{"date":"2020-12-25T17:22:02Z","dateType":"Submitted"},{"date":"2021-01-12T00:00:00Z","dateType":"Issued"},{"date":"2021-01-12T00:00:00Z","dateType":"Available"}],"language":"en","types":{"ris":"DATA","bibtex":"misc","citeproc":"dataset","schemaOrg":"Dataset","resourceType":"dataset","resourceTypeGeneral":"Dataset"},"relatedIdentifiers":[{"relationType":"IsCitedBy","relatedIdentifier":"10.1063/1.5099487","relatedIdentifierType":"DOI"}],"relatedItems":[],"sizes":["12534129 bytes"],"formats":[],"version":"3","rightsList":[{"rights":"Creative Commons Zero v1.0 Universal","rightsUri":"https://creativecommons.org/publicdomain/zero/1.0/legalcode","schemeUri":"https://spdx.org/licenses/","rightsIdentifier":"cc0-1.0","rightsIdentifierScheme":"SPDX"}],"descriptions":[{"description":"Real-time optical reflection of incident p-polarized light near\n Brewster’s angle shows that after drop-casting iron oxide nanoparticles\n (NPs) in heptane on top of a diethylene glycol (DEG) liquid substrate, an\n iron oxide NP layer forms at the DEG/heptane interface, and it self-limits\n to a monolayer even when there are excess NPs dispersed in the upper\n heptane phase. Most modes of NP self-assembly do not self-limit growth\n after the formation of a single monolayer. Observations are compared to a\n reflection model incorporating the reflectances expected at each\n interface. An effective medium model of the dielectric constant is used to\n model the reflectance of the NP layer at the DEG/heptane interface.","descriptionType":"Abstract"},{"description":"To form these NP assemblies, 2 mL of DEG were first deposited\n into a glass Petri dish (diameter = 3.45 cm) to form a ∼2.14 mm-thick\n liquid substrate (if the surface were flat).\n A \u003ci\u003ep\u003c/i\u003e-polarized He-Ne laser (632.8 nm, plasma filter) was\n expanded from below to form a 2.21 cm × 1.32 cm elliptical beam at the\n center of the DEG/air interface, to average over this region, and all\n reflected beams other than those from the glass bottom of the Petri dish\n were imaged on a photodiode, on which they overlap. The laser was adjusted\n to hit the DEG/air interface at Brewster’s angle (34.65°) to minimize\n reflectance from this interface. Then, 1400 μL of heptane were deposited\n on the DEG substrate to form a ∼1.50 mm-thick upper layer reservoir and,\n finally, 120 μL of a heptane colloid of NPs were drop-cast on top. This\n quickly mixed with the heptane reservoir to form a more dilute, ∼1.63\n mm-thick heptane colloid layer. The Petri dish was then capped to slow the\n heptane evaporation. The NPs were spherical iron oxide NPs\n (Fe\u003csub\u003e2\u003c/sub\u003eO\u003csub\u003e3\u003c/sub\u003e, 11.8 nm core\n diameter, capped by oleate) synthesized by standard methods. The number of\n NPs in the heptane colloid drop was characterized by the number of\n close-packed NP MLs that would be expected to form on the DEG substrate\n after heptane evaporation, averaged over the surface; this is termed the\n number of ML-equivalents being drop-cast. The light\n beams reflected from the DEG/heptane colloid and heptane colloid/air\n interfaces were monitored by a photodiode for 240 min, way before the\n heptane upper layer evaporated. Before the heptane was added, the\n reflected fraction from the DEG/air interface was very small, but not\n zero, because of the surface and laser beam curvatures. After it was added\n and before the NPs were drop-cast, the reflectances from the DEG/heptane\n and heptane/air interfaces were still very small because the refractive\n indices of pure DEG and heptane are nearly the same (below). After the NPs\n were added and a NP layer formed at the DEG/heptane colloid interface, the\n reflectance from that interface was expected to initially increase\n monotonically and linearly with layer thickness at the interface (for up\n to ∼6 MLs, corresponding to ∼ a quarter wavelength in this\n medium).","descriptionType":"Methods"}],"geoLocations":[],"fundingReferences":[{"schemeUri":"https://ror.org","funderName":"National Science Foundation","awardNumber":"CBET-1603043","funderIdentifier":"https://ror.org/021nxhr62","funderIdentifierType":"ROR"},{"schemeUri":"https://ror.org","funderName":"National Science Foundation","awardNumber":"DGE-1069240","funderIdentifier":"https://ror.org/021nxhr62","funderIdentifierType":"ROR"}],"xml":"<?xml version="1.0" encoding="UTF-8"?>
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  <identifier identifierType="DOI">10.5061/DRYAD.V9S4MW6TM</identifier>
  <creators>
    <creator>
      <creatorName nameType="Personal">Hu, Jiayang</creatorName>
      <nameIdentifier nameIdentifierScheme="ORCID" schemeURI="http://orcid.org/">0000-0001-6707-1549</nameIdentifier>
      <affiliation affiliationIdentifier="https://ror.org/00hj8s172" affiliationIdentifierScheme="ROR" schemeURI="https://ror.org">Columbia University</affiliation>
    </creator>
    <creator>
      <creatorName nameType="Personal">Pan, Brady</creatorName>
      <affiliation affiliationIdentifier="https://ror.org/00hj8s172" affiliationIdentifierScheme="ROR" schemeURI="https://ror.org">Columbia University</affiliation>
    </creator>
    <creator>
      <creatorName nameType="Personal">Makihara, Takuma</creatorName>
      <affiliation affiliationIdentifier="https://ror.org/008zs3103" affiliationIdentifierScheme="ROR" schemeURI="https://ror.org">Rice University</affiliation>
    </creator>
    <creator>
      <creatorName nameType="Personal">Garcia, Roy D. J.</creatorName>
      <affiliation affiliationIdentifier="https://ror.org/00hj8s172" affiliationIdentifierScheme="ROR" schemeURI="https://ror.org">Columbia University</affiliation>
    </creator>
    <creator>
      <creatorName nameType="Personal">Herman, Irving P.</creatorName>
      <affiliation affiliationIdentifier="https://ror.org/00hj8s172" affiliationIdentifierScheme="ROR" schemeURI="https://ror.org">Columbia University</affiliation>
    </creator>
  </creators>
  <titles>
    <title>
      Brewster angle optical reflection observation of self-limiting
      nanoparticle monolayer self-assembly at a liquid/liquid interface
    </title>
  </titles>
  <publisher publisherIdentifier="https://ror.org/00x6h5n95" publisherIdentifierScheme="ROR" schemeURI="https://ror.org/">Dryad</publisher>
  <resourceType resourceTypeGeneral="Dataset">dataset</resourceType>
  <publicationYear>2021</publicationYear>
  <subjects>
    <subject subjectScheme="fos" schemeURI="https://web-archive.oecd.org/2012-06-15/138575-38235147.pdf">FOS: Nano-technology</subject>
  </subjects>
  <fundingReferences>
    <fundingReference>
      <funderName>National Science Foundation</funderName>
      <funderIdentifier funderIdentifierType="ROR">https://ror.org/021nxhr62</funderIdentifier>
      <awardNumber>CBET-1603043</awardNumber>
    </fundingReference>
    <fundingReference>
      <funderName>National Science Foundation</funderName>
      <funderIdentifier funderIdentifierType="ROR">https://ror.org/021nxhr62</funderIdentifier>
      <awardNumber>DGE-1069240</awardNumber>
    </fundingReference>
  </fundingReferences>
  <dates>
    <date dateType="Submitted">2020-12-25T17:22:02Z</date>
    <date dateType="Issued">2021-01-12T00:00:00Z</date>
    <date dateType="Available">2021-01-12T00:00:00Z</date>
  </dates>
  <language>en</language>
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  </rightsList>
  <descriptions>
    <description descriptionType="Abstract">
      Real-time optical reflection of incident&amp;nbsp;p-polarized light near
      Brewster’s angle shows that after drop-casting iron oxide nanoparticles
      (NPs) in heptane on top of a diethylene glycol (DEG) liquid substrate, an
      iron oxide NP layer forms at the DEG/heptane interface, and it self-limits
      to a monolayer even when there are excess NPs dispersed in the upper
      heptane phase. Most modes of NP self-assembly do not self-limit growth
      after the formation of a single monolayer. Observations are compared to a
      reflection model incorporating the reflectances expected at each
      interface. An effective medium model of the dielectric constant is used to
      model the reflectance of the NP layer at the DEG/heptane interface.
    </description>
    <description descriptionType="Methods">
      &lt;p&gt;To form these NP assemblies, 2 mL of DEG were first deposited
      into a glass Petri dish (diameter = 3.45 cm) to form a ∼2.14 mm-thick
      liquid substrate (if the surface were flat).
      A &lt;i&gt;p&lt;/i&gt;-polarized He-Ne laser (632.8 nm, plasma filter) was
      expanded from below to form a 2.21 cm × 1.32 cm elliptical beam at the
      center of the DEG/air interface, to average over this region, and all
      reflected beams other than those from the glass bottom of the Petri dish
      were imaged on a photodiode, on which they overlap. The laser was adjusted
      to hit the DEG/air interface at Brewster’s angle (34.65°) to minimize
      reflectance from this interface. Then, 1400 μL of heptane were deposited
      on the DEG substrate to form a ∼1.50 mm-thick upper layer reservoir and,
      finally, 120 μL of a heptane colloid of NPs were drop-cast on top. This
      quickly mixed with the heptane reservoir to form a more dilute, ∼1.63
      mm-thick heptane colloid layer. The Petri dish was then capped to slow the
      heptane evaporation. The NPs were spherical iron oxide NPs
      (Fe&lt;sub&gt;2&lt;/sub&gt;O&lt;sub&gt;3&lt;/sub&gt;, 11.8 nm core
      diameter, capped by oleate) synthesized by standard methods. The number of
      NPs in the heptane colloid drop was characterized by the number of
      close-packed NP MLs that would be expected to form on the DEG substrate
      after heptane evaporation, averaged over the surface; this is termed the
      number of ML-equivalents being drop-cast.&lt;/p&gt; &lt;p&gt;The light
      beams reflected from the DEG/heptane colloid and heptane colloid/air
      interfaces were monitored by a photodiode for 240 min, way before the
      heptane upper layer evaporated. Before the heptane was added, the
      reflected fraction from the DEG/air interface was very small, but not
      zero, because of the surface and laser beam curvatures. After it was added
      and before the NPs were drop-cast, the reflectances from the DEG/heptane
      and heptane/air interfaces were still very small because the refractive
      indices of pure DEG and heptane are nearly the same (below). After the NPs
      were added and a NP layer formed at the DEG/heptane colloid interface, the
      reflectance from that interface was expected to initially increase
      monotonically and linearly with layer thickness at the interface (for up
      to ∼6 MLs, corresponding to ∼ a quarter wavelength in this
      medium).&lt;/p&gt;
    </description>
  </descriptions>
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