{"data":{"id":"10.5061/dryad.79cnp5ht5","type":"dois","attributes":{"doi":"10.5061/dryad.79cnp5ht5","prefix":"10.5061","suffix":"dryad.79cnp5ht5","identifiers":[],"alternateIdentifiers":[],"creators":[{"name":"Zhang, Fang","nameType":"Personal","givenName":"Fang","familyName":"Zhang","affiliation":["Beijing University of Technology"],"nameIdentifiers":[{"schemeUri":"https://orcid.org","nameIdentifier":"https://orcid.org/0000-0003-1908-3865","nameIdentifierScheme":"ORCID"}]},{"name":"Wang, Qi","nameType":"Personal","givenName":"Qi","familyName":"Wang","affiliation":["Beijing University of Technology"],"nameIdentifiers":[]},{"name":"Li, Wenjing","nameType":"Personal","givenName":"Wenjing","familyName":"Li","affiliation":["Beijing University of Technology"],"nameIdentifiers":[]},{"name":"Shang, Hui","nameType":"Personal","givenName":"Hui","familyName":"Shang","affiliation":["Beijing University of Technology"],"nameIdentifiers":[]},{"name":"Bai, Shiyang","nameType":"Personal","givenName":"Shiyang","familyName":"Bai","affiliation":["Beijing University of Technology"],"nameIdentifiers":[]},{"name":"Sun, Jihong","nameType":"Personal","givenName":"Jihong","familyName":"Sun","affiliation":["Beijing University of Technology"],"nameIdentifiers":[]}],"titles":[{"title":"pH-sensitive thiamethoxam nanoparticles based on bimodal mesoporous silica for improving insecticidal efficiency"}],"publisher":"Dryad","container":{},"publicationYear":2020,"subjects":[{"subject":"FOS: Nano-technology","schemeUri":"https://web-archive.oecd.org/2012-06-15/138575-38235147.pdf","subjectScheme":"fos"}],"contributors":[],"dates":[{"date":"2020-12-23T09:40:08Z","dateType":"Submitted"},{"date":"2020-12-26T00:00:00Z","dateType":"Issued"},{"date":"2020-12-26T00:00:00Z","dateType":"Available"}],"language":"en","types":{"ris":"DATA","bibtex":"misc","citeproc":"dataset","schemaOrg":"Dataset","resourceType":"dataset","resourceTypeGeneral":"Dataset"},"relatedIdentifiers":[{"relationType":"IsCitedBy","relatedIdentifier":"10.1098/rsos.201967","relatedIdentifierType":"DOI"}],"relatedItems":[],"sizes":["8086701 bytes"],"formats":[],"version":"2","rightsList":[{"rights":"Creative Commons Zero v1.0 Universal","rightsUri":"https://creativecommons.org/publicdomain/zero/1.0/legalcode","schemeUri":"https://spdx.org/licenses/","rightsIdentifier":"cc0-1.0","rightsIdentifierScheme":"SPDX"}],"descriptions":[{"description":"In this study, we synthesized pH-sensitive\n thiamethoxam-3-(2-aminoethylamino) propyl-bimodal mesoporous silica\n (P/Thi-NN-BMMs) nanoparticles (NPs). We used this bimodal mesoporous\n silica (BMMs) mesoporous material as a carrier based on the principle of\n free radical polymerization. The size of the P/Thi-NN-BMMs NPs was about\n 891.7±4.9 nm, with a zeta potential of about −25.7±2.5 mV. X-ray\n powder diffraction (XRPD) analysis, N2-sorption measurements, and\n thermogravimetric (TG) analysis indicated that thiamethoxam (Thi) was\n loaded into the pores of the mesoporous structure and that the mesopore\n surface was coated with polyacrylic acid (PAA). The loading rate of\n P/Thi-NN-BMMs was about 25.2%. The controlled-release NPs had excellent\n anti-photolysis performance and storage stability. The NPs showed\n significant pH sensitivity, and the Thi release rate in pH 10.0 phosphate\n buffer was higher than those in pH 7.4 and pH 3.0 phosphate buffers. We\n described the sustained-release curves according to the Weibull model. The\n relative toxicity of P/Thi-NN-BMMs against peach aphid was 1.44 times that\n of commercial Thi. This provides a promising instrument for effective\n insect control and environment protection.","descriptionType":"Abstract"},{"description":"Particle size distributions of BMMs, NN-BMMs, P/NN-BMMs and\n P/Thi-NN-BMMs were displayed in Fig. 3. We determined particle size,\n polymer dispersity index (PDI), and zeta potential of BMMs, NN-BMMs,\n P/NN-BMMs,and P/Thi-NN-BMMs according to dynamic light scattering (DLS)\n using the Zetasizer Nano ZS (Malvern Instruments Ltd., Malvern,\n UK). XRPD patterns, TG curves,\n N\u003csub\u003e2\u003c/sub\u003e adsorption/desorption isotherms, and BET surface\n areas and pore volumes of P/Thi-NN-BMMs and the control samples were\n displayed in Fig 4. We performed X-ray powder diffraction on an X-ray\n powder diffractometer (D8 ADVANCE X, Bruker/AXS, Karlsruhe, Germany) using\n nickel-filtered Cu Kα radiation (λ = 0.154 nm). The tube voltage and tube\n current were 35 kV and 35 mA, respectively, and the scan speed was 0.5\n min\u003csup\u003e-1  \u003c/sup\u003e(Fig 4A). We conducted TG analysis using a\n thermal analyzer (PerkinElmer, Waltham, MA, USA), under the following\n conditions: nitrogen atmosphere, a flow rate of 20\n mLmin\u003csup\u003e-1\u003c/sup\u003e, and a heating rate of 10 °C\n min\u003csup\u003e-1\u003c/sup\u003e; the highest temperature was 800 °C. The\n pesticide loading content of the P/Thi-NN-BMMs nano-pesticide was\n calculated according to the TG curve(Fig 4B). We obtained nitrogen\n adsorption-desorption isotherms on an Autosorb-iQ pore analyzer\n (Quantachrome, Boynton Beach, FL, USA) at 77 K under continuous adsorption\n conditions. Brunauer-Emmett-Teller (BET) and used Barrett-Joyner-Halenda\n analyses to calculate the surface area, pore size, and pore volume(Fig 4C,\n 4D). Photodegradation curves of\n P/Thi-NN-BMMs Nps and technical Thi under UV irradiation were displayed in\n Fig. 5. We tested the photolytic properties of P/Thi-NN-BMMs\n NPs with technical Thi as the control. The samples were divided equally\n into culture dishes and irradiated under a UV lamp (500 W) at a distance\n of 20 cm in a UV-light incubator (WFH-203B, Shanghai Precision Instrument\n Co., Ltd., Shanghai, China). At a given irradiation time (12, 24, 36, 48,\n 60, 72, and 96 h), we separately collected the culture dishes and analyzed\n the Thi contents in the samples by high-performance liquid chromatography\n (HPLC). A gradient of methanol–water(40:60) was programmed over 30 min at\n a flow rate of 1 mL min\u003csup\u003e-1\u003c/sup\u003e with detection at 240 nm.\n We performed all experiments in triplicate. Stability of P/Thi-NN-BMMs NPs at\n different storage temperatures after 14 days were displayed in Fig. 6. We\n determined the stability of the P/Thi-NN-BMMs NPs according to CIPAC MT 46\n (Miscellaneous Techniques and Impurities: MT 46 Accelerated Storage\n Procedure, Collaborative International Pesticides Analytical Council) and\n GB/T 19136–2003 (Determination of Heat Storage Stability of Pesticides,\n Chinese National Standard). We stored the samples at 4 ± 2 °C and 25 ± 2\n °C for 7 d and 54 ± 2 °C for 14 d, and analyzed the Thi content using\n HPLC. Cumulative\n release profiles of P/Thi-NN-BMMs with pH of 3.0, 7.4, and\n 10.0 were displayed in Fig. 7. we suspended 30 mg of\n P/Thi-NN-BMMs  in 100 mL of an ethanol:water mixture (30:70, v/v), which\n was used as the release medium. Then, we collected 2 mL of the sample for\n testing at fixed time intervals, and the system was replenished with an\n equal amount of fresh medium. We measured Thi concentrations using HPLC\n and calculated the release rate of Thi from the nano-delivery sample. The\n liquid-phase detection conditions included a mobile phase of\n methanol:water (volume ratio 40:60), injection volume of 10 μL, wavelength\n of 240 nm, and retention time of 4 min.","descriptionType":"Methods"},{"description":"Someone can use this dataset directly, and there are no missing\n values.","descriptionType":"Other"}],"geoLocations":[],"fundingReferences":[{"schemeUri":"https://ror.org","funderName":"Ministry of Science and Technology of the People's Republic of China","awardNumber":"2016YFD0200502-2","funderIdentifier":"https://ror.org/027s68j25","funderIdentifierType":"ROR"}],"xml":"<?xml version="1.0" encoding="UTF-8"?>
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  <identifier identifierType="DOI">10.5061/DRYAD.79CNP5HT5</identifier>
  <creators>
    <creator>
      <creatorName nameType="Personal">Zhang, Fang</creatorName>
      <nameIdentifier nameIdentifierScheme="ORCID" schemeURI="http://orcid.org/">0000-0003-1908-3865</nameIdentifier>
      <affiliation affiliationIdentifier="https://ror.org/037b1pp87" affiliationIdentifierScheme="ROR" schemeURI="https://ror.org">Beijing University of Technology</affiliation>
    </creator>
    <creator>
      <creatorName nameType="Personal">Wang, Qi</creatorName>
      <affiliation affiliationIdentifier="https://ror.org/037b1pp87" affiliationIdentifierScheme="ROR" schemeURI="https://ror.org">Beijing University of Technology</affiliation>
    </creator>
    <creator>
      <creatorName nameType="Personal">Li, Wenjing</creatorName>
      <affiliation affiliationIdentifier="https://ror.org/037b1pp87" affiliationIdentifierScheme="ROR" schemeURI="https://ror.org">Beijing University of Technology</affiliation>
    </creator>
    <creator>
      <creatorName nameType="Personal">Shang, Hui</creatorName>
      <affiliation affiliationIdentifier="https://ror.org/037b1pp87" affiliationIdentifierScheme="ROR" schemeURI="https://ror.org">Beijing University of Technology</affiliation>
    </creator>
    <creator>
      <creatorName nameType="Personal">Bai, Shiyang</creatorName>
      <affiliation affiliationIdentifier="https://ror.org/037b1pp87" affiliationIdentifierScheme="ROR" schemeURI="https://ror.org">Beijing University of Technology</affiliation>
    </creator>
    <creator>
      <creatorName nameType="Personal">Sun, Jihong</creatorName>
      <affiliation affiliationIdentifier="https://ror.org/037b1pp87" affiliationIdentifierScheme="ROR" schemeURI="https://ror.org">Beijing University of Technology</affiliation>
    </creator>
  </creators>
  <titles>
    <title>
      pH-sensitive thiamethoxam nanoparticles based on bimodal mesoporous silica
      for improving insecticidal efficiency
    </title>
  </titles>
  <publisher publisherIdentifier="https://ror.org/00x6h5n95" publisherIdentifierScheme="ROR" schemeURI="https://ror.org/">Dryad</publisher>
  <resourceType resourceTypeGeneral="Dataset">dataset</resourceType>
  <publicationYear>2020</publicationYear>
  <subjects>
    <subject subjectScheme="fos" schemeURI="https://web-archive.oecd.org/2012-06-15/138575-38235147.pdf">FOS: Nano-technology</subject>
  </subjects>
  <fundingReferences>
    <fundingReference>
      <funderName>Ministry of Science and Technology of the People's Republic of China</funderName>
      <funderIdentifier funderIdentifierType="ROR">https://ror.org/027s68j25</funderIdentifier>
      <awardNumber>2016YFD0200502-2</awardNumber>
    </fundingReference>
  </fundingReferences>
  <dates>
    <date dateType="Submitted">2020-12-23T09:40:08Z</date>
    <date dateType="Issued">2020-12-26T00:00:00Z</date>
    <date dateType="Available">2020-12-26T00:00:00Z</date>
  </dates>
  <language>en</language>
  <relatedIdentifiers>
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    <rights rightsURI="https://spdx.org/licenses/CC0-1.0.html">Creative Commons Zero v1.0 Universal</rights>
  </rightsList>
  <descriptions>
    <description descriptionType="Abstract">
      In this study, we synthesized pH-sensitive
      thiamethoxam-3-(2-aminoethylamino) propyl-bimodal mesoporous silica
      (P/Thi-NN-BMMs) nanoparticles (NPs). We used this bimodal mesoporous
      silica (BMMs) mesoporous material as a carrier based on the principle of
      free radical polymerization. The size of the P/Thi-NN-BMMs NPs was about
      891.7±4.9&amp;nbsp;nm, with a zeta potential of about −25.7±2.5 mV. X-ray
      powder diffraction (XRPD) analysis, N2-sorption measurements, and
      thermogravimetric (TG) analysis indicated that thiamethoxam (Thi) was
      loaded into the pores of the mesoporous structure and that the mesopore
      surface was coated with polyacrylic acid (PAA). The loading rate of
      P/Thi-NN-BMMs was about 25.2%. The controlled-release NPs had excellent
      anti-photolysis performance and storage stability. The NPs showed
      significant pH sensitivity, and the Thi release rate in pH 10.0 phosphate
      buffer was higher than those in pH 7.4 and pH 3.0 phosphate buffers. We
      described the sustained-release curves according to the Weibull model. The
      relative toxicity of P/Thi-NN-BMMs against peach aphid was 1.44 times that
      of commercial Thi. This provides a promising instrument for effective
      insect control and environment protection.
    </description>
    <description descriptionType="Methods">
      &lt;p&gt;Particle size distributions of BMMs, NN-BMMs, P/NN-BMMs and
      P/Thi-NN-BMMs were displayed in Fig. 3. We determined particle size,
      polymer dispersity index (PDI), and zeta potential of BMMs, NN-BMMs,
      P/NN-BMMs,and P/Thi-NN-BMMs according to dynamic light scattering (DLS)
      using the Zetasizer Nano ZS (Malvern Instruments Ltd., Malvern,
      UK).&lt;/p&gt; &lt;p&gt;XRPD patterns, TG curves,
      N&lt;sub&gt;2&lt;/sub&gt; adsorption/desorption isotherms, and BET surface
      areas and pore volumes of P/Thi-NN-BMMs and the control samples were
      displayed in Fig 4. We performed X-ray powder diffraction on an X-ray
      powder diffractometer (D8 ADVANCE X, Bruker/AXS, Karlsruhe, Germany) using
      nickel-filtered Cu Kα radiation (λ = 0.154 nm). The tube voltage and tube
      current were 35 kV and 35 mA, respectively, and the scan speed was 0.5
      min&lt;sup&gt;-1  &lt;/sup&gt;(Fig 4A). We conducted TG analysis using a
      thermal analyzer (PerkinElmer, Waltham, MA, USA), under the following
      conditions: nitrogen atmosphere, a flow rate of 20
      mLmin&lt;sup&gt;-1&lt;/sup&gt;, and a heating rate of 10 °C
      min&lt;sup&gt;-1&lt;/sup&gt;; the highest temperature was 800 °C. The
      pesticide loading content of the P/Thi-NN-BMMs nano-pesticide was
      calculated according to the TG curve(Fig 4B). We obtained nitrogen
      adsorption-desorption isotherms on an Autosorb-iQ pore analyzer
      (Quantachrome, Boynton Beach, FL, USA) at 77 K under continuous adsorption
      conditions. Brunauer-Emmett-Teller (BET) and used Barrett-Joyner-Halenda
      analyses to calculate the surface area, pore size, and pore volume(Fig 4C,
      4D).&lt;/p&gt; &lt;p
      style="text-align:justify;"&gt;Photodegradation curves of
      P/Thi-NN-BMMs Nps and technical Thi under UV irradiation were displayed in
      Fig. 5. &lt;span&gt;We tested the photolytic properties of P/Thi-NN-BMMs
      NPs with technical Thi as the control. The samples were divided equally
      into culture dishes and irradiated under a UV lamp (500 W) at a distance
      of 20 cm in a UV-light incubator (WFH-203B, Shanghai Precision Instrument
      Co., Ltd., Shanghai, China). At a given irradiation time (12, 24, 36, 48,
      60, 72, and 96 h), we separately collected the culture dishes and analyzed
      the Thi contents in the samples by high-performance liquid chromatography
      (HPLC). A gradient of methanol–water(40:60) was programmed over 30 min at
      a flow rate of 1 mL min&lt;sup&gt;-1&lt;/sup&gt; with detection at 240 nm.
      We performed all experiments in triplicate.&lt;/span&gt;&lt;/p&gt; &lt;p
      style="text-align:justify;"&gt;Stability of P/Thi-NN-BMMs NPs at
      different storage temperatures after 14 days were displayed in Fig. 6. We
      determined the stability of the P/Thi-NN-BMMs NPs according to CIPAC MT 46
      (Miscellaneous Techniques and Impurities: MT 46 Accelerated Storage
      Procedure, Collaborative International Pesticides Analytical Council) and
      GB/T 19136–2003 (Determination of Heat Storage Stability of Pesticides,
      Chinese National Standard). We stored the samples at 4 ± 2 °C and 25 ± 2
      °C for 7 d and 54 ± 2 °C for 14 d, and analyzed the Thi content using
      HPLC.&lt;/p&gt; &lt;p style="text-align:justify;"&gt;&lt;span
      lang="EN-US" style="background:white;"&gt;Cumulative
      release profiles of P/Thi-NN-BMMs with pH of 3.0, 7.4, and
      10.0 &lt;/span&gt;were displayed in Fig. 7. we suspended 30 mg of
      P/Thi-NN-BMMs  in 100 mL of an ethanol:water mixture (30:70, v/v), which
      was used as the release medium. Then, we collected 2 mL of the sample for
      testing at fixed time intervals, and the system was replenished with an
      equal amount of fresh medium. We measured Thi concentrations using HPLC
      and calculated the release rate of Thi from the nano-delivery sample. The
      liquid-phase detection conditions included a mobile phase of
      methanol:water (volume ratio 40:60), injection volume of 10 μL, wavelength
      of 240 nm, and retention time of 4 min.&lt;/p&gt;
    </description>
    <description descriptionType="Other">
      &lt;p&gt;Someone can use this dataset directly, and there are no missing
      values.&lt;/p&gt;
    </description>
  </descriptions>
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